1-Butyne, 3-chloro-3-methyl- → (1,1-Dimethyl-prop-2-ynyl)-(2-methoxy-ethyl)-methyl-amine

HRID 270439Notes

Reaction equation

HRID 270439 reaction equation
Cl[C:2]([CH3:6])([CH3:5])[C:3]#[CH:4].[CH3:7][O:8][CH2:9][CH2:10][NH:11][CH3:12]>>[CH3:5][C:2]([N:11]([CH2:10][CH2:9][O:8][CH3:7])[CH3:12])([CH3:6])[C:3]#[CH:4]

Participants

3

Reactant 2

HCID 706791-Butyne, 3-chloro-3-methyl-HCID 300977(2-Methoxyethyl)(methyl)amine

Product 1

HCID 22314051(1,1-Dimethyl-prop-2-ynyl)-(2-methoxy-ethyl)-methyl-amine

Procedure

In analogy to example 37.1, 3-Chloro-3-methyl-1-butyne and N-(2-Methoxyethyl)methylamine were converted to yield (1,1-Dimethyl-prop-2-ynyl)-(2-methoxy-ethyl)-methyl-amine as colorless oil, MS: 155 (M).

Sources & evidence

ORD record
ord-e0aa63cae60546d68934b6b1f2264f42
Source dataset
uspto-grants-2008_11
Patent number
US07449483B2

Reaction notes

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