3-Butyn-2-ol → HCID 22314084, compound
Reaction equation
[CH3:1][CH:2](O)[C:3]#[CH:4].[CH3:6][O:7][CH2:8][CH2:9][NH:10][CH2:11][CH3:12]>>[CH2:11]([N:10]([CH2:9][CH2:8][O:7][CH3:6])[CH:2]([CH3:1])[C:3]#[CH:4])[CH3:12]Participants
3
Procedure
In analogy to example 37.5 and 37.6, 3-Butyn-2-ol and N-(Methoxyethyl)ethylamine were converted to yield Ethyl-(2-methoxy-ethyl)-(1-methyl-prop-2-ynyl)-amine as colorless oil, MS: 155 (M).
Sources & evidence
- ORD record
- ord-a85c39fb7dff44159c8715bf7e8f1e71
- Source dataset
- uspto-grants-2008_11
- Patent number
- US07449483B2
Reaction notes
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