HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22313915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophene | HCID 22313940 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 22313915 | HCID 22313915 | — |
Reaction Steps
In analogy to the method described in example 17.1, 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophene (example 27.5) was treated with methylamine in ethanol and N,N-dimethylacetamide to yield {4-[3-(4-Bromo-phenyl)-2-methyl-benzo[b]thiophen-6-yloxy]-butyl}-methyl-amine as colorless oil, MS: 405 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449483B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-e5932368927a4f55b5a5e039408e5211 |
| Source note | uspto-grants-2008_11 |