DI-1-Adamantylphosphinic chloride → Di-1-adamantylphosphine

HRID 270737Notes

Reaction equation

HRID 270737 reaction equation
[C:1]12([PH:11](=O)[C:12]34[CH2:21][CH:16]5[CH2:17][CH:18]([CH2:20][CH:14]([CH2:15]5)[CH2:13]3)[CH2:19]4)[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.C12(P(Cl)(C34CC5CC(CC(C5)C3)C4)=O)CC3CC(CC(C3)C1)C2>>[C:1]12([PH:11][C:12]34[CH2:13][CH:14]5[CH2:15][CH:16]([CH2:17][CH:18]([CH2:20]5)[CH2:19]3)[CH2:21]4)[CH2:2][CH:3]3[CH2:9][CH:7]([CH2:6][CH:5]([CH2:4]3)[CH2:10]1)[CH2:8]2

Participants

3

Reactant 2

HCID 5191267DI-1-Adamantylphosphinic chlorideHCID 178527023HCID 178527023, compound

Product 1

HCID 11077518Di-1-adamantylphosphine

Procedure

This example illustrates the formation of di-1-adamantylphosphine oxide from di-1-adamantylphosphinic chloride in two steps, the first step resulting in the formation of di-1-adamantylphosphine.

Sources & evidence

ORD record
ord-e77f2c4c003e4e1e8b9eb01e24014579
Source dataset
uspto-grants-2008_11
Patent number
US07449601B2

Reaction notes

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