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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 270752Generated: October 29, 2026

Water → HCID 69279913, compound

https://huagongshe.com/reaction/270752

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantMethyl iodideHCID 6328—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 69279508HCID 69279508—
SolventDimethylformamideHCID 6228—
ProductHCID 69279913HCID 6927991382.8%

Reaction Steps

3.6 g of 2-hydroxy-6-n-dodecyl aminocarbonylnaphthalene obtained in example 2 was dissolved in 36 g of dimethylformamide. To this solution, 1.7 g of potassium carbonate and 2.2 g of methyl iodide were added, and allowed to react at 40° C. for 8 hours. The reaction liquid was poured to 180 g of water, and then precipitate was filtrated, washed thoroughly with methanol and water, dried to give 3.1 g of 2-methoxy-6-n-dodecyl aminocarbonylnaphthalene (Decomposition point: 324° C.). The infrared absorption spectrum (KBr) of the compound is shown in FIG. 3. The triboelectric charge was measured by blow-off method as described in example 1. The triboelectric charge of the compound was +17.6 μC/g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07449608B2
Source datasetuspto-grants-2008_11
ORD IDord-edca22e00e6447ff99dcb0821953e700
Source noteuspto-grants-2008_11