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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 27093Generated: October 25, 2026

Methylamine → HCID 178484399, compound

https://huagongshe.com/reaction/27093

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
Reactant1,1-Bis(methylthio)-2-nitroethyleneHCID 83623—
ReactantHCID 178503827HCID 178503827—
ReactantHCID 178511474HCID 178511474—
ProductHCID 178484399HCID 178484399—

Reaction Steps

4-[2-(2-Aminoethylthio)ethyl]imidazole (from the dihydrobromide (4.0 g)) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) by the procedure of Example 8(i) and the resultant 1-nitro-2-methylthio-2-[2-(2-(4-imidazolyl)ethylthio)ethylamino]ethylene is treated with methylamine according to the procedure of Example 8(ii) to yield the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04220652
Source datasetuspto-grants-1980_09
ORD IDord-f782c24fb68c4ba0869769d710c7de27
Source noteuspto-grants-1980_09