HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178484396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | HCID 178503822 | HCID 178503822 | — |
| Reactant | HCID 178510963 | HCID 178510963 | — |
| Product | HCID 178484396 | HCID 178484396 | — |
Reaction Steps
When 5-bromo-4-(4-aminobutyl)imidazole is reacted with 1-nitro2,2-bis-methylthioethylene according to the procedure of Example 8(i) and the resultant 1-nitro-2-methylthio-2-[4-(5-bromo-4-imidazolyl)butylamino]ethylene, m.p. 157°-158° treated with methylamine by the procedure of Example 8(ii), the title compound, m.p. 145°-148° is produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04220652 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-d37836d45ca448d58edf0e9818e7f0c4 |
| Source note | uspto-grants-1980_09 |