HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Iodide Ion
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 58714336 | HCID 58714336 | — |
| Product | Iodide Ion | HCID 30165 | — |
| Product | HCID 178504133 | HCID 178504133 | — |
Reaction Steps
To neat (2R)-N-(4-chlorophenyl)-4-methylthio-2-[(phenylmethoxy)carbonylamino]butanamide (2.0 g, 5.09 mmol) was added methyl iodide (10 ml, 161 mmol). The solution was allowed to stir for 48 hours. Methyl iodide was then removed under vacuum to yield (2R)-N-(4-chlorophenyl)-5-methyl-2-[(phenylmethoxy)carbonylamino]-5-thiahexanamide, iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452889B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-82f5c276b0b94866a7457d1e6fa23773 |
| Source note | uspto-grants-2008_11 |