Sodium Hydroxide → HCID 178525478, compound

HRID 27131Notes

Reaction equation

[C:1]([CH2:4][CH2:5][CH2:6][NH:7][C:8](=[S:11])SC)([OH:3])=[O:2].[N-:12]=[N+:13]=[N-:14].[Na+].[OH-].[Na+]>>[C:1]([CH2:4][CH2:5][CH2:6][N:7]1[C:8]([SH:11])=[N:14][N:13]=[N:12]1)([OH:3])=[O:2]

Participants

Reactant 3

HCID 14798Sodium Hydroxide

HCID 33557Sodium Azide

HCID 12458602Methyl 3-carboxypropyldithiocarbamate

Product 1

HCID 178525478HCID 178525478, compound

Procedure

Reaction of methyl 3-carboxypropyldithiocarbamate with sodium azide and sodium hydroxide as described in Example 7 gave 1-(3-carboxypropyl)tetrazole-5-thiol, m.p. 99°-101°.

Sources & evidence

ORD record: ord-5d17208dd89443a4851501ee90e10f8c
Source dataset: uspto-grants-1980_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04220644

Reaction notes

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