Sodium Hydroxide → HCID 178525438, compound

HRID 27132Notes

Reaction equation

[C:1]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:10](=[S:13])SC)([OH:3])=[O:2].[N-:14]=[N+:15]=[N-:16].[Na+].[OH-].[Na+]>>[C:1]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][N:9]1[C:10]([SH:13])=[N:16][N:15]=[N:14]1)([OH:3])=[O:2]

Participants

Reactant 3

HCID 14798Sodium Hydroxide

HCID 33557Sodium Azide

HCID 12458604Methyl 5-carboxypentyldithiocarbamate

Product 1

HCID 178525438HCID 178525438, compound

Procedure

Reaction of methyl 5-carboxypentyldithiocarbamate with sodium azide and sodium hyroxide as described in Example 7 gave 1-(5-carboxypentyl)tetrazole-5-thiol, m.p. 100°-100.5°.

Sources & evidence

ORD record: ord-8d03a2879e3c467797534302fa9d8a62
Source dataset: uspto-grants-1980_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04220644

Reaction notes

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