HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 178524540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 178498353 | HCID 178498353 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178524540 | HCID 178524540 | — |
Reaction Steps
The mixture of 110 mg of 2,6-dichloro-4-tetrazolylbenzoic acid methylester, 0.5 ml of dichloromethane solution containing 1M BBr3 and 5 ml of dichloromethane was stirred overnight. The obtained substance was treated by an ordinary method using dichloromethane as an extractant and purified by reverse phase HPLC to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452905B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-7d90a62e74e149149d7097e71d20000e |
| Source note | uspto-grants-2008_11 |