5-(chloromethyl)-2-methylpyridine hydrochloride → HCID 67247855, compound

HRID 271489Notes

Reaction equation

HRID 271489 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:15])[NH:13][CH:14]=2)[CH:5]=[CH:4][N:3]=1.Cl.Cl[CH2:18][C:19]1[CH:20]=[CH:21][C:22]([CH3:25])=[N:23][CH:24]=1>>[CH3:25][C:22]1[CH:21]=[CH:20][C:19]([CH2:18][N:13]2[CH:14]=[C:10]([C:9]#[C:8][C:6]3[CH:5]=[CH:4][N:3]=[C:2]([CH3:1])[CH:7]=3)[N:11]=[C:12]2[CH3:15])=[CH:24][N:23]=1

Participants

3

Reactant 2

HCID 122143395-(chloromethyl)-2-methylpyridine hydrochlorideHCID 178418884HCID 178418884, compound

Product 1

HCID 67247855HCID 67247855, compound

Procedure

The title compound, MS: m/e=303.2 (M+H30), was prepared in accordance with the general method of example 1 from 2-methyl-4-(2-methyl-1H-imidazol-4-ylethynyl)-pyridine and 5-chloromethyl-2-methyl-pyridine hydrochloride.

Sources & evidence

ORD record
ord-f31171c4f6bb42dbb72743b827d40899
Source dataset
uspto-grants-2008_11
Patent number
US07452909B2

Reaction notes

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