(1-Bromoethyl)benzene → HCID 67246294, compound
Reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:15])[NH:13][CH:14]=2)[CH:5]=[CH:4][N:3]=1.Br[CH:17]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH3:18]>>[CH3:1][C:2]1[CH:7]=[C:6]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:15])[N:13]([CH:17]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH3:18])[CH:14]=2)[CH:5]=[CH:4][N:3]=1Participants
3
Procedure
The title compound, MS: m/e=302.2 (M+H30), was prepared in accordance with the general method of example 1 from 2-methyl-4-(2-methyl-1H-imidazol-4-ylethynyl)-pyridine and (1-bromoethyl)benzene.
Sources & evidence
- ORD record
- ord-833604f65d7542e4814134f6e34f83fe
- Source dataset
- uspto-grants-2008_11
- Patent number
- US07452909B2
Reaction notes
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