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HRID271856

反应详情

EQUATION

反应方程式

HRID 271856 的结构方程式

REACTANTS

反应物

3
结构：O=S(=O)([O-])C(F)(F)F
HCID2758875

Trifluoromethanesulfonate

CF3O3S-

结构：CCOC(=O)[C@H](Cc1ccc(OS(=O)(=O)C(F)(F)F)cc1)NC(=O)OC(C)(C)C
HCID10789275

未命名化合物

结构：COC(=O)[C@](Cc1ccc(O)cc1)(N=C=O)OC(C)(C)C
HCID86601622

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@@H](Cc1ccc(OS(=O)(=O)C(F)(F)F)cc1)NC(=O)OC(C)(C)C
HCID53983472

未命名化合物

收率 91%

PROCEDURE

实验过程

In a manner similar to the preparation of ethyl (S)-2-tert-butoxycarbonylamino-3-(4-trifluoromethanesulfonyloxyphenyl)propionate (Example 1b), using 25 g (84.7 mmol) of methyl (R)-2-tert-butoxy-carbonylamino-3-(4-hydroxyphenyl)propionate, 33 g of triflate are isolated with a 91% yield.

WORKUP

后处理

  1. customare isolated with a 91% yield