HCID 20434624, compound → 1-(2,6-Dichlorophenyl)-1-methylguanidine

HRID 27194Notes

Reaction equation

HRID 27194 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[N:10]([CH3:14])[C:11]([NH2:13])=[NH:12]>[OH-].[Na+]>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[N:10]([CH3:14])[C:11]([NH2:13])=[NH:12]

Participants

3

Reactant 1

HCID 20434624HCID 20434624, compound

Product 1

HCID 204345371-(2,6-Dichlorophenyl)-1-methylguanidine

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

The free base is prepared by dissolving 1-(2,6-dichlorophenyl)-1-methylguanidine hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 1-(2,6-dichlorophenyl)-1-methylguanidine.

Workup

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

Sources & evidence

ORD record
ord-fb0348f84e864d8ebaa27fba61802f0a
Source dataset
uspto-grants-1980_09
Patent number
US04220658

Reaction notes

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