HCID 23148931, compound → HCID 23148929, compound

Participants

Reaction Steps

This solution was dropped into a solution of 4.11 g (15.7 mmol) of (2-indenyl)(diisopropylamino)chloroborane in 30 ml of tetrahydrofuran at 0° C. After stirring at room temperature for four hours, the solvent was evaporated and the residue was extracted twice with 40 ml of hexane and 10 ml of dichloromethane to obtain 6.47 g (19.0 mmol) of bis(2-indenyl)(diisopropylamino)borane as a pale yellow solid.

Provenance & Evidence