HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl isocyanate → HCID 140327414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl isocyanate | HCID 62412 | — |
| Reactant | 1-(2,6-Dichlorophenyl)-1-methylguanidine | HCID 20434537 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 140327414 | HCID 140327414 | — |
Reaction Steps
To a mixture of 10.9 g (0.05 mole) of 1-(2,6-dichlorophenyl)-1-methylguanidine and 10 ml xylene is added 5 g of t-butylisocyanate (0.05 mole) and the mixture is refluxed for 2 hours. The reaction product is cooled, triturated with heptane and filtered. Recrystallization from 1:1 isopropanol/water results in 1-(2,6-dichlorophenyl-N-methylamidino)-3-(t-butyl)urea.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04220658 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-c71b5cebe52a4aeca891b59a6e0ff344 |
| Source note | uspto-grants-1980_09 |