HCID 20434628, compound → HCID 20434629, compound

HRID 27204Notes

Reaction equation

HRID 27204 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:14][C:15]([NH2:17])=[O:16])=[N:12][CH3:13]>[OH-].[Na+]>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:14][C:15]([NH2:17])=[O:16])=[N:12][CH3:13]

Participants

3

Reactant 1

HCID 20434628HCID 20434628, compound

Product 1

HCID 20434629HCID 20434629, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

The free base is prepared by dissolving the above hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 1-(2,6-dichlorophenyl-N'-methylamidino)urea.

Workup

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

Sources & evidence

ORD record
ord-e423da3e0b1c48fd9839d8e6b92afbd5
Source dataset
uspto-grants-1980_09
Patent number
US04220658

Reaction notes

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