HRID27217

反应详情

EQUATION

反应方程式

HRID 27217 的结构方程式

PROCEDURE

实验过程

3-Methylthio-6-(3-methoxybenzyl)-1,2,4-triazin-5-one (1.18 g) and 2-(2-thiazolylmethylthio)ethylamine (0.87 g) were heated together on an oil bath (160°-70°) for 3/4 hour. The resulting oil, after chromatography and crystallisation from ethanol, gave the title compound as a colourless solid (0.83 g) m.p. 128°-29°.

WORKUP

后处理

  1. customThe resulting oil, after chromatography and crystallisation from ethanol