Thionyl Chloride → Butanoyl chloride, 2-(3-pentadecylphenoxy)-

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Reaction Steps

2-(3-Pentadecylphenoxy)butanoic acid (4.18 g, 0.01 mol) (CAS Registry Number 14230-52-5) and thionyl chloride (30 ml) were heated under reflux on a steam-bath for 1 h. The resulting yellow solution was allowed to cool before being distilled under reduced pressure to leave a yellow oil. The oil was dissolved in dichloromethane (50 ml) and the solution was distilled under reduced pressure to remove volatiles. The residual 2-(3-pentadecylphenoxy)butanoyl chloride was used without further purification.

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