HCID 21961327, compound → HCID 21961366, compound

HRID 272332Notes

Reaction equation

HRID 272332 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[C:7](=O)[N:6]([C:13]1[C:14]([CH3:35])=[C:15]([CH3:34])[C:16]3[O:20][C:19]([CH3:22])([CH3:21])[CH:18]([C:23]4[CH:28]=[CH:27][C:26]([CH:29]([CH3:31])[CH3:30])=[CH:25][CH:24]=4)[C:17]=3[C:32]=1[CH3:33])[C:5]2=O>CCCCCC>[Cl:11][C:10]1[CH:9]=[C:8]2[C:4](=[CH:3][C:2]=1[Cl:1])[CH2:5][N:6]([C:13]1[C:14]([CH3:35])=[C:15]([CH3:34])[C:16]3[O:20][C:19]([CH3:21])([CH3:22])[CH:18]([C:23]4[CH:28]=[CH:27][C:26]([CH:29]([CH3:31])[CH3:30])=[CH:25][CH:24]=4)[C:17]=3[C:32]=1[CH3:33])[CH2:7]2

Participants

3

Reactant 1

HCID 21961327HCID 21961327, compound

Product 1

HCID 21961366HCID 21961366, compoundYield 16%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

By using 5,6-dichloro-2-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione, the title compound was synthesized according to Example 2a. Yield: 16%. Melting point: 148-150° C. (Hexane)

Sources & evidence

ORD record
ord-7ac12064008f425d8bd6a9e253981bac
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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