Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 272352Generated: October 31, 2026

Benzene, (3-chloro-1-propenyl)- → HCID 21961361, compound

https://huagongshe.com/reaction/272352

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, (3-chloro-1-propenyl)-HCID 94242—
ReactantN-(4-hydroxy-2,3,6-trimethylphenyl)formamideHCID 21961295—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 21961361HCID 2196136144%

Reaction Steps

By using N-(4-hydroxy-2,3,6-trimethylphenyl)formamide and cinnamyl chloride, the title compound was synthesized according to Reference Example 17b. Yield: 44%. Melting point: 197-199° C. (Ethyl acetate-hexane)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07456162B2
Source datasetuspto-grants-2008_11
ORD IDord-d3c1ab33cd4c4e4ea5da0b5e4cf29922
Source noteuspto-grants-2008_11