HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenylacetyl chloride → HCID 10276991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenylacetyl chloride | HCID 2734688 | — |
| Reactant | 3-(4-Isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine | HCID 10519978 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10276991 | HCID 10276991 | 74% |
Reaction Steps
By using 3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine and 4-methoxyphenylacetyl chloride, the title compound was synthesized according to Example 1b. Yield: 74%. Melting point: 171-173° C. (Methanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456162B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-87b5eba243674ba49291b101482a83c0 |
| Source note | uspto-grants-2008_11 |