HCID 10276991, compound → HCID 9933828, compound

HRID 272371Notes

Reaction equation

HRID 272371 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:33])=[C:16]([NH:21][C:22](=O)[CH2:23][C:24]4[CH:29]=[CH:28][C:27]([O:30][CH3:31])=[CH:26][CH:25]=4)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2([CH3:35])[CH3:34])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>CCCCCC>[CH:1]([C:4]1[CH:5]=[CH:6][C:7]([CH:10]2[C:14]3[C:15]([CH3:33])=[C:16]([NH:21][CH2:22][CH2:23][C:24]4[CH:25]=[CH:26][C:27]([O:30][CH3:31])=[CH:28][CH:29]=4)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2([CH3:35])[CH3:34])=[CH:8][CH:9]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 10276991HCID 10276991, compound

Product 1

HCID 9933828HCID 9933828, compoundYield 66%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

By using N-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-4-methoxyphenylacetamide, the title compound was synthesized according to Example 2b. Yield: 66%. Melting point: 63-65° C. (Hexane)

Sources & evidence

ORD record
ord-fafd1abee2c44a9592e396c77dc82456
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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