HCID 21961320, compound → HCID 68437955, compound

HRID 272378Notes

Reaction equation

HRID 272378 reaction equation
[Cl:1][C:2]1[CH:33]=[CH:32][C:5]([C:6]([NH:8][C:9]2[C:10]([CH3:31])=[C:11]([CH3:30])[C:12]3[O:16][C:15]([CH3:18])([CH3:17])[CH:14]([C:19]4[CH:24]=[CH:23][C:22]([CH:25]([CH3:27])[CH3:26])=[CH:21][CH:20]=4)[C:13]=3[C:28]=2[CH3:29])=O)=[CH:4][CH:3]=1>CO>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][NH:8][C:9]2[C:10]([CH3:31])=[C:11]([CH3:30])[C:12]3[O:16][C:15]([CH3:17])([CH3:18])[CH:14]([C:19]4[CH:24]=[CH:23][C:22]([CH:25]([CH3:26])[CH3:27])=[CH:21][CH:20]=4)[C:13]=3[C:28]=2[CH3:29])=[CH:32][CH:33]=1

Participants

3

Reactant 1

HCID 21961320HCID 21961320, compound

Product 1

HCID 68437955HCID 68437955, compoundYield 37%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

By using 4-chloro-N-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]benzamide, the title compound was synthesized according to Example 2b. Yield: 37%. Melting point: 93-94° C. (Methanol)

Sources & evidence

ORD record
ord-5197fc6b518744a890669eb23ca95b43
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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