HCID 10181308, compound → HCID 10112805, compound

HRID 272384Notes

Reaction equation

HRID 272384 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[C:12]3[C:13]([CH3:30])=[C:14]([NH:19][C:20](=O)[C:21]4[CH:26]=[CH:25][C:24]([O:27][CH3:28])=[CH:23][CH:22]=4)[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][C:9]2([CH3:32])[CH3:31])=[CH:4][CH:3]=1>CO>[F:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]2[C:12]3[C:13]([CH3:30])=[C:14]([NH:19][CH2:20][C:21]4[CH:22]=[CH:23][C:24]([O:27][CH3:28])=[CH:25][CH:26]=4)[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][C:9]2([CH3:32])[CH3:31])=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 10181308HCID 10181308, compound

Product 1

HCID 10112805HCID 10112805, compoundYield 52%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

By using N-[3-(4-fluorophenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-4-methoxybenzamide, the title compound was synthesized according to Example 2b. Yield: 52%. Melting point: 114-115° C. (Methanol)

Sources & evidence

ORD record
ord-84eef54e4e664f29a9fcbd178c2bee33
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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