HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzoyl chloride → HCID 10273713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | HCID 10828013 | HCID 10828013 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 10273713 | HCID 10273713 | 75% |
Reaction Steps
By using 3-(4-fluorophenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine and 4-fluorobenzoyl chloride, the title compound was synthesized according to Example 1b. Yield: 75%. Melting point: 140-142° C. (Ethyl acetate-hexane)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456162B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-5d47792070b84eeba4c5a200a72d5685 |
| Source note | uspto-grants-2008_11 |