4-Fluoro-N-(2,4,6,7-tetramethyl-3-phenyl-5-benzofuranyl)benzamide → HCID 10292741, compound

HRID 272394Notes

Reaction equation

HRID 272394 reaction equation
[F:1][C:2]1[CH:29]=[CH:28][C:5]([C:6]([NH:8][C:9]2[C:10]([CH3:27])=[C:11]([CH3:26])[C:12]3[O:16][C:15]([CH3:17])=[C:14]([C:18]4[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=4)[C:13]=3[C:24]=2[CH3:25])=O)=[CH:4][CH:3]=1>CO>[F:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][NH:8][C:9]2[C:10]([CH3:27])=[C:11]([CH3:26])[C:12]3[O:16][C:15]([CH3:17])=[C:14]([C:18]4[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=4)[C:13]=3[C:24]=2[CH3:25])=[CH:28][CH:29]=1

Participants

3

Reactant 1

HCID 102935794-Fluoro-N-(2,4,6,7-tetramethyl-3-phenyl-5-benzofuranyl)benzamide

Product 1

HCID 10292741HCID 10292741, compoundYield 56%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

By using 4-fluoro-N-(2,4,6,7-tetramethyl-3-phenyl-1-benzofuran-5-yl)benzamide, the title compound was synthesized according to Example 2b. Yield: 56%. Melting point: 135-136° C. (Methanol).

Sources & evidence

ORD record
ord-afe9752b28d54fd1b5cf99d5098325c8
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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