HCID 10202077, compound → HCID 10222836, compound

HRID 272402Notes

Reaction equation

HRID 272402 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[C:13]([CH3:30])=[C:14]([NH:19][C:20](=O)[C:21]4[CH:26]=[CH:25][C:24]([O:27][CH3:28])=[CH:23][CH:22]=4)[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][C:9]=2[CH3:31])=[CH:4][CH:3]=1>C(O)C>[CH3:28][O:27][C:24]1[CH:23]=[CH:22][C:21]([CH2:20][NH:19][C:14]2[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]3[O:10][C:9]([CH3:31])=[C:8]([C:5]4[CH:6]=[CH:7][C:2]([F:1])=[CH:3][CH:4]=4)[C:12]=3[C:13]=2[CH3:30])=[CH:26][CH:25]=1

Participants

3

Reactant 1

HCID 10202077HCID 10202077, compound

Product 1

HCID 10222836HCID 10222836, compoundYield 75%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

By using N-[3-(4-fluorophenyl)-2,4,6,7-tetramethyl-1-benzofuran-5-yl]-4-methoxybenzamide, the title compound was synthesized according to Example 2b. Yield: 75%. Melting point: 100-102° C. (Ethanol).

Sources & evidence

ORD record
ord-a8fec4ad5c6f4a5a9d986407b7bafbb8
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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