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HRID272456

反应详情

EQUATION

反应方程式

HRID 272456 的结构方程式

REACTANTS

反应物

2
结构：Cc1c(I)c(=O)n(C2CCCC2)c2nc(S(C)=O)ncc12
HCID11212220

8-Cyclopentyl-6-iodo-2-methanesulfinyl-5-methyl-8H-pyrido[2,3-d]pyrimidin-7-one

C14H16IN3O2S

结构：CSc1ncc2cc(Br)c(=O)n(C3CCCC3)c2n1
HCID22329765

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)c1ncc2cc(Br)c(=O)n(C3CCCC3)c2n1
HCID11428232

未命名化合物

PROCEDURE

实验过程

Prepared from 6-bromo-8-cyclopentyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one following the procedure described for 8-cyclopentyl-6-iodo-2-methanesulfinyl-5-methyl-8H-pyrido[2,3-d]pyrimidin-7-one. MS (APCI) Calc'd for C13H14BrN3O2S: 357, 355.0. Found: 358 (M+1), 356. 1H NMR δ (400 MHz, DMSO-d6) 9.14 (s, 1H), 8.63 (s, 1H), 5.91-5.86 (m, 1H), 2.89 (s, 3H), 2.15 (br s, 2H), 2.04 (br s, 2H), 1.87-1.79 (m, 2H), 1.61-1.58 (m, 2H).