Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Sulfuryl chloride | HCID 24648 | — |
| 반응물 | 2-(2-Benzoyloxyethoxyimino)-3-oxobutyrate | HCID 86737192 | — |
| 생성물 | Ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate | HCID 53906646 | — |
반응 단계
A solution of 2-(2-benzoyloxyethoxyimino)-3-oxobutyrate (syn isomer, 28 g.), sulfuryl chloride (13.5 g.) and acetic acid (30 ml.) was stirred at 40° C. for 10 minutes and at room temperature for 5.5 hrs. The reaction mixture was treated in a conventional manner to give ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate (syn isomer, 29 g.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220761 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-543dacb9fc1340ff993e4c9130a635d3 |
| 출처 메모 | uspto-grants-1980_09 |