HRID27320
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (2.0 g) is dissolved in toluene and an excess of anhydrous dimethylamine is bubbled into the reaction mixture, the solvent removed in vacuo and the residue triturated with cold diethyl ether to give 1.1 g of product.
WORKUP
后处理
- customan excess of anhydrous dimethylamine is bubbled into the reaction mixture
- customthe solvent removed in vacuo
- customthe residue triturated with cold diethyl ether