反应详情

4 ml (126 mmol) of hydrazine are added to 600 mg (2.2 mmol) of 4′-chloro-[2,2′;6′,2″]-terpyridine in 12 ml of 2-butanol. The mixture is heated at reflux for 17 hours and cooled, and [2,2′;6′,2″]terpyridin-4′-yl-hydrazine is filtered off in the form of a white solid.

1. temperatureThe mixture is heated
2. temperatureat reflux for 17 hours
3. temperaturecooled
4. filtration[2,2′;6′,2″]terpyridin-4′-yl-hydrazine is filtered off in the form of a white solid