Ethanolamine → HCID 14666852, compound

HRID 273366Notes

Reaction equation

HRID 273366 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([F:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[NH2:12][CH2:13][CH2:14][OH:15]>>[F:8][C:5]1[CH:6]=[CH:7][C:2]([NH:12][CH2:13][CH2:14][OH:15])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 677672,5-Difluoronitrobenzene

Product 1

HCID 14666852HCID 14666852, compound

Procedure

This compound was prepared from 1,4-difluoro-2-nitrobenzene (21.8 ml, 100 mmol) and 2-amino ethanol (10 ml, 300 mmol) using analogous procedure described in Step A of Example 3. Yield (19.2 g, 96%).

Workup

  1. customYield (19.2 g, 96%)

Sources & evidence

ORD record
ord-e404e416bb5244bea1de727a63fbc6bf
Source dataset
uspto-grants-2008_11
Patent number
US07456293B2

Reaction notes

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