Thiophosgene → HCID 54372553、化合物

関与物質

反応手順

2,4-Dichloroaniline (0.85 g) was allowed to react with thiophosgen (0.4 ml), followed by the reaction with (2R,3R)-2-(2,4-difluorophenyl)-3-mercapto-1-[1H-1,2,4-triazol-1-yl]-2-butanol (0.5 g) by the same manner as in Example 5. The compound (23), i.e., [(2R,3R)-3-(2,4-difluorophenyl)-3-hydroxy-4-(1H-1,2,4-triazol-1-yl)-2-butyl] N-(2,4-dichlorophenyl)dithiocarbamate (0.08 g) was obtained as a pale yellow oil.

情報源と証拠