Allyl Alcohol → HCID 57258425, compound

HRID 273882Notes

Reaction equation

[CH2:1]([OH:4])[CH:2]=[CH2:3].[CH3:5][O:6][CH:7]([O:10][CH3:11])[CH2:8]Br>>[CH3:5][O:6][CH:7]([O:10][CH3:11])[CH2:8][O:4][CH2:1][CH:2]=[CH2:3]

Participants

Reactant 2

HCID 7858Allyl Alcohol

HCID 816722-Bromo-1,1-dimethoxyethane

Product 1

HCID 57258425HCID 57258425, compound

Procedure

Perkin Elmer 8310 GC (8% carbowax+2% KOH on chromasorb 80-100 mesh, 80°-200° C. in 20 min. Product retention 5.775 minutes, allyl alcohol 3.61 min, bromo-acetaldehyde dimethyl acetal 5.44 min. FID detection.

Sources & evidence

ORD record: ord-f592e77ce0334115bda457ca19867fa8
Source dataset: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05387692

Reaction notes

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