HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylvanillin → HCID 54235796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylvanillin | HCID 8467 | — |
| Reactant | 4(5H)-Thiazolone, 3-(dimethylamino)dihydro-2-thioxo- | HCID 4341978 | — |
| Product | HCID 54235796 | HCID 54235796 | 59.3% |
Reaction Steps
3-Ethoxy-4-hydroxybenzaldehyde (45.7 g), N-dimethylaminorhodanine (53.35 g) and fused sodium acetate (92.4 g) were reacted in the manner described in Example 1 to provide 52.92 g of the subtitled intermediate. m.p. 194°-198° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05387690 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-b4f5aa06ecce4ad1afe5327d9feee4a7 |
| Source note | uspto-grants-1995_02 |