HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride → HCID 10579044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride | HCID 6456035 | — |
| Reactant | HCID 19042068 | HCID 19042068 | — |
| Product | HCID 10579044 | HCID 10579044 | 51.6% |
Reaction Steps
The procedure of Example 3 is repeated using 4.3 g of α-(5-chlorohexyl)-3,4-dimethoxy-α-[(4-methylphenyl)thio]benzeneacetonitrile and 4.25 g of 6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride. This affords 3.05 g of the desired product as a golden gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05387685 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-495033569c034010bca577e4bbc1afcb |
| Source note | uspto-grants-1995_02 |