HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Acetylimidazolidinone → 3-(2-imidazolin-2-ylamino)-2,3,4,5-tetrahydro-1H-3-benzazepin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Acetylimidazolidinone | HCID 79350 | — |
| Reactant | 3-amino-2,3,4,5-tetrahydro-1H-3-benzazepin | HCID 12931570 | — |
| Product | 3-(2-imidazolin-2-ylamino)-2,3,4,5-tetrahydro-1H-3-benzazepin | HCID 23342921 | — |
Reaction Steps
5 g of (0.03 M) 3-amino-2,3,4,5-tetrahydro-1H-3-benzazepin and 4.3 g of (0.034 M) 1-acetyl-imidazolidin-2-one are stirred in 50 ml POCL3 for 1 hour at 100° C. The remaining process steps are analogous to those set forth in Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221798 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-ca09b85885634a7d906c54626f6893d9 |
| Source note | uspto-grants-1980_09 |