HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178447866, compound → HCID 178447867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178447866 | HCID 178447866 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178447867 | HCID 178447867 | — |
Reaction Steps
A solution of 12.6 g of 3-[4-(trans-4-propyl-cyclohexyl)-phenyl]-propenoic acid (obtained by condensation of 4-(trans-4-propylcyclohexyl)-benzaldehyde with malonic acid in pyridine) in 120 ml of ethyl acetate is hydrogenated at room temperature and atmospheric pressure, using 4 g of Pd/C (5% Pd) as catalyst. The catalyst is filtered off, and the filtrate is evaporated. Colourless crystals are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389292 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-006afb2fe33c445f9d9762aeb4ae8cd7 |
| Source note | uspto-grants-1995_02 |