HCID 20092191, compound → HCID 20092190, compound

HRID 274190Notes

Reaction equation

HRID 274190 reaction equation
[CH3:1][C:2]([CH2:8][C:9]([CH3:12])([CH3:11])[CH3:10])([CH2:6][OH:7])[C:3](O)=[O:4].C([O-])([O-])(OC)CC>>[CH3:1][C:2]1([CH2:8][C:9]([CH3:12])([CH3:11])[CH3:10])[CH2:6][O:7][C:3]1=[O:4]

Participants

3

Reactant 2

HCID 20092191HCID 20092191, compoundHCID 86748448HCID 86748448, compound

Product 1

HCID 20092190HCID 20092190, compound

Procedure

The resultant 2-methyl-2-neopentyl-3-hydroxypropionic acid (2.) was then reacted conventionally with methyl orthopropionate, followed by slow heating in the presence of Amberlyst® 15, then worked up to obtained the desired final product.

Workup

  1. temperatureby slow heating in the presence of Amberlyst® 15

Sources & evidence

ORD record
ord-db5d81ba296448508164311af7e44f6e
Source dataset
uspto-grants-1995_02
Patent number
US05389447

Reaction notes

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