Pyrogallol → HCID 20092283, compound

HRID 274198Notes

Reaction equation

HRID 274198 reaction equation
[C:1]1([CH:9]=[CH:8][CH:7]=[C:5]([OH:6])[C:3]=1[OH:4])[OH:2].[CH:10]([O:13][CH2:14]Cl)([CH3:12])[CH3:11]>>[CH:10]([O:13][CH2:14][O:2][C:1]1[CH:9]=[CH:8][CH:7]=[C:5]([O:6][CH2:14][O:13][CH:10]([CH3:12])[CH3:11])[C:3]=1[O:4][CH2:14][O:13][CH:10]([CH3:12])[CH3:11])([CH3:12])[CH3:11]

Participants

3

Reactant 2

HCID 1057PyrogallolHCID 124317162-(Chloromethoxy)propane

Product 1

HCID 20092283HCID 20092283, compound

Procedure

Using pyrogallol in place of phloroglucinol used in Synthesis Example 13 and isopropoxymethylchloride obtained in Synthesis Example 2, the reaction and treatment were carried out in the same manner as described in Synthesis Example 13 to give the corresponding 1,2,3-tris(isopropoxymethoxy)benzene as a yellow oil.

Workup

  1. customobtained in Synthesis Example 2
  2. customthe reaction and treatment
  3. customas described in Synthesis Example 13

Sources & evidence

ORD record
ord-44542bb48004437da041e3641dfd9e29
Source dataset
uspto-grants-1995_02
Patent number
US05389491

Reaction notes

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