6-Chloro-7-methyl-[1,2,4]triazolo[1,5-b]pyridazine → 1-Hexanesulfonamide, 3,3-dimethyl-6-((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)-

HRID 274276Notes

Reaction equation

HRID 274276 reaction equation
CN(C=[N:5][S:6]([CH2:9][CH2:10][C:11]([CH3:17])([CH3:16])[CH2:12][CH2:13][CH2:14][OH:15])(=[O:8])=[O:7])C.Cl[C:19]1[C:20]([CH3:28])=[CH:21][C:22]2[N:23]([N:25]=[CH:26][N:27]=2)[N:24]=1>>[CH3:17][C:11]([CH3:16])([CH2:10][CH2:9][S:6](=[O:7])(=[O:8])[NH2:5])[CH2:12][CH2:13][CH2:14][O:15][C:19]1[C:20]([CH3:28])=[CH:21][C:22]2[N:23]([N:25]=[CH:26][N:27]=2)[N:24]=1

Participants

3

Reactant 2

HCID 118051586-Chloro-7-methyl-[1,2,4]triazolo[1,5-b]pyridazineHCID 53714418HCID 53714418, compound

Product 1

HCID 30737941-Hexanesulfonamide, 3,3-dimethyl-6-((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)-

Procedure

Using 6-(N,N-dimethylaminomethylene)aminosulfonyl-4,4-dimethyl-1-hexanol and 6-chloro-7-methyl[1,2,4]triazolo[1,5-b]pyridazine, the same reaction as in Example 6 was conducted to produce the title compound. m.p. 154°-155° C.

Workup

  1. customthe same reaction as in Example 6

Sources & evidence

ORD record
ord-e270bc87f46f42c580db21c0f0088026
Source dataset
uspto-grants-1995_02
Patent number
US05389633

Reaction notes

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