6-Chloro-2,7-dimethyl[1,2,4]triazolo[1,5-b]pyridazine → 1-Butanesulfonamide, 2-(((2,7-dimethyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-2-ethyl-

HRID 274279Notes

Reaction equation

HRID 274279 reaction equation
CN(C=[N:5][S:6]([CH2:9][C:10]([CH2:15][CH3:16])([CH2:13][CH3:14])[CH2:11][OH:12])(=[O:8])=[O:7])C.Cl[C:18]1[C:19]([CH3:28])=[CH:20][C:21]2[N:22]([N:24]=[C:25]([CH3:27])[N:26]=2)[N:23]=1>>[CH2:15]([C:10]([CH2:13][CH3:14])([CH2:9][S:6](=[O:7])(=[O:8])[NH2:5])[CH2:11][O:12][C:18]1[C:19]([CH3:28])=[CH:20][C:21]2[N:22]([N:24]=[C:25]([CH3:27])[N:26]=2)[N:23]=1)[CH3:16]

Participants

3

Reactant 2

HCID 107261326-Chloro-2,7-dimethyl[1,2,4]triazolo[1,5-b]pyridazineHCID 536426363-(N,N-dimethylaminomethylene)aminosulfonyl-2,2-diethyl-1-propanol

Product 1

HCID 30737971-Butanesulfonamide, 2-(((2,7-dimethyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-2-ethyl-

Procedure

Using 3-(N,N-dimethylaminomethylene)aminosulfonyl-2,2-diethyl-1-propanol and 6-chloro-2,7-dimethyl[1,2,4]triazolo[1,5-b]pyridazine, the same reaction as in Example 6 was conducted to produce the title compound. m.p. 221°-222° C.

Workup

  1. customthe same reaction as in Example 6

Sources & evidence

ORD record
ord-bdd88dfc9bc244c4b3bd41185ad8d6ac
Source dataset
uspto-grants-1995_02
Patent number
US05389633

Reaction notes

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