1-Bromo-2-Chloroethane → Ethyl 4-chloro-2,2-diethylbutyrate

HRID 274291Notes

Reaction equation

HRID 274291 reaction equation
[CH2:1]([CH:3]([CH2:9][CH3:10])[C:4]([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].Br[CH2:12][CH2:13][Cl:14]>>[Cl:14][CH2:13][CH2:12][C:3]([CH2:9][CH3:10])([CH2:1][CH3:2])[C:4]([O:6][CH2:7][CH3:8])=[O:5]

Participants

3

Reactant 2

HCID 78491-Bromo-2-ChloroethaneHCID 76326Ethyl 2-ethylbutyrate

Product 1

HCID 10512495Ethyl 4-chloro-2,2-diethylbutyrate

Procedure

Using ethyl 2-ethylbutyrate and 1-bromo-2-chloroethane, the same reaction as in Reference Example 16 was conducted to produce the title compound. b.p. 69°-72° C./0.3 mmHg

Workup

  1. customthe same reaction as in Reference Example 16

Sources & evidence

ORD record
ord-a5a538a6c7b34f7eb58104d1699de5d8
Source dataset
uspto-grants-1995_02
Patent number
US05389633

Reaction notes

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