HCID 23342827, compound → HCID 23342835, compound

HRID 27431Notes

Reaction equation

HRID 27431 reaction equation
[N+:1]([C:4]1[CH:17]=[CH:16][C:7]([CH2:8][CH:9]2[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][NH:10]2)=[CH:6][CH:5]=1)([O-])=O>C(O)C.[Pt].[H][H]>[NH2:1][C:4]1[CH:17]=[CH:16][C:7]([CH2:8][CH:9]2[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][NH:10]2)=[CH:6][CH:5]=1

Participants

4

Reactant 1

HCID 23342827HCID 23342827, compound

Product 1

HCID 23342835HCID 23342835, compound

Reagents, catalysts & solvents 2

HCID 178506450HCID 178506450, compoundCatalystHCID 702EthanolSolvent

Procedure

Hydrogenate 12 g of the title compound of Example 16 in 300 ml of ethyl alcohol with platinum/hydrogen. After the absorption of hydrogen has ceased, filter off the catalyst and concentrate the filtrate to obtain 10.5 g (100% of theory) of the title compound as a dark brown viscous oil.

Workup

  1. customAfter the absorption of hydrogen
  2. filtrationfilter off the catalyst
  3. concentrationconcentrate the filtrate

Sources & evidence

ORD record
ord-087fb5902b1e4a958e6d696f71f5352e
Source dataset
uspto-grants-1980_09
Patent number
US04221788

Reaction notes

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