HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 15239119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 15239125 | HCID 15239125 | — |
| Reactant | HCID 178527880 | HCID 178527880 | — |
| Product | HCID 15239119 | HCID 15239119 | — |
Reaction Steps
Generally following the procedure of Example 7, 2-mercapto-2-thiazoline (0.67 g, 5.6 mmol) is treated with sodium hydride (0.35 g, 7.3 mmol), with cooling, and the resulting sodium salt is reacted with 1-methyl-2-[4-(1methylpropylthio)phenoxy]ethyl bromide (1.70 g, 5.6 mmol) at RT to give 2-{1-methyl-2-[4-(1-methylpropylthio)phenoxy]ethylthio}-2-thiazoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389651 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-e8df4daf53eb4aa58097930efe075e3b |
| Source note | uspto-grants-1995_02 |