HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20093207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 15764662 | HCID 15764662 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20093207 | HCID 20093207 | — |
Reaction Steps
A mixture of 2-(4-isopropoxyphenoxy)ethanol (3.50 g), mesyl chloride (2.20 g) and triethylamine (2.0 g) in 20 ml of methylene chloride is stirred at RT for 3 hours. It is then poured into water and extracted with methylene chloride. The solvent is removed from the combined organic layers by rotoevaporation, and the residue is purified by column chromatography to give 2-(4-isopropoxyphenoxy)ethyl methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389651 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-e31084d6e3eb4654aa53ae108c255c01 |
| Source note | uspto-grants-1995_02 |