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Acetaldehyde → alpha-Methyl-1-(2-methylpropyl)-1H-imidazo[4,5-c]quinoline-2-methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetaldehyde | HCID 177 | — |
| 反応物 | Deaminoimiquimod | HCID 11424651 | — |
| 生成物 | alpha-Methyl-1-(2-methylpropyl)-1H-imidazo[4,5-c]quinoline-2-methanol | HCID 15224403 | — |
反応手順
Using the general method of Example 45, 1-(2-methylpropyl)-1H-imidazo[4,5-c]quinoline (20 g; 89 mmol) was reacted with acetaldehyde to provide the desired product. The structure was confirmed by nuclear magnetic resonance spectroscopy.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05389640 |
| 出典データセット | uspto-grants-1995_02 |
| ORD ID | ord-7f7c4d2d823e431082a27a56a2a51d3b |
| 出典メモ | uspto-grants-1995_02 |