HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycolic Acid → HCID 15224455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycolic Acid | HCID 757 | — |
| Reactant | HCID 13958330 | HCID 13958330 | — |
| Product | HCID 15224455 | HCID 15224455 | 78.3% |
Reaction Steps
Using the general method of Example 1, N-butyl-3-nitro-4-quinolinamine (9.8 g, 0.04 mole, Example 122) was hydrogenated then reacted with glycolic acid (9.1 g, 0.12 mole) to provide 8.0 g of the desired product as a solid. A small sample was recrystallized from ethyl acetate to provide pure material, m.p. 146°-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389640 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-1a4c8b79433b40ff83ce7f2d6f0bc92b |
| Source note | uspto-grants-1995_02 |